Sintering of translucent and single-phase nanostructured scandia-stabilized zirconia
Abstract: Fully-dense and single-phase nanostructured scandia-stabilized zirconia specimens were produced by high-pressure spark plasma sintering technique. Nanocrystalline powders were prepared by the copre-cipitation method. Green pellets were sintered at temperatures varying from 700 to 900 degrees C and pressures from 1.4 to 2 GPa, resulting in dense microstructures with single-phase fluorite-type cubic structure within a wide range of Sc2O3 content (6-15 mol%). The average grain size of sintered specimens ranged from 8 to 20 nm. Transmittance spectra confirm translucence in sintered specimens, which is consistent with full density. The results reported here reveal that the polymorphism challenge in the zirconia-scandia system can be successfully suppressed by this consolidation technique, which allows for controlling the grain size of bulk specimens.
Author(s): Grosso, RL; Muche, DNF; Yonamine, T; Muccillo, ENS ; Dillon, SJ ; Castro, RHR
MATERIALS LETTERS
Volume: 253 Published: OCT 15 2019
DOI: 10.1016/j.matlet.2019.06.076
