SEM, AFM and TEM images of LNO films sintered by (a,b,e) conventional (LNO-A) and (c,d,f) microwave (LNO-B) heating sources
Role of morphological characteristics on the conductive behavior of LaNiO3 thin films
Abstract: LaNiO3 (LNO) thin films were synthesized via the polymeric precursor method and sintered using conventional and microwave heating sources. The samples were characterized by structural morphological and electrical techniques. The crystalline structure was analyzed by X-ray diffraction and indicated rhombohedral perovskite phase in both films sintered using conventional and microwave heating. The films morphology was evaluated by scanning and transmission electron microscopy, and atomic force microscopy, and the results point out that microwave heating exerts direct influence on the morphological characteristics of LNO films contributing towards the change in the grain size distribution, porosity and roughness. Conductivity was also investigated through four-probe measurements, which pointed out a conductive and ohmic behavior of the LNO thin films prepared via the polymeric precursor method where a direct relationship was found between the morphological characteristics and the electrical properties of LNO film. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
O Laboratório Aberto de Interatividade para Disseminação do Conhecimento Científico e Tecnológico (LAbI), vinculado à Universidade Federal de São Carlos (UFSCar), é voltado à prática da divulgação científica pautada na interatividade; nas relações entre Ciência, Arte e Tecnologia.
Writers: Marco A. L. Cordeiro, Edson R. Leite, and Eric A. Stach Keywords: Nanoparticle; Structure Abstract: The tailoring of nanoparticle superlattices is fundamental to the design of novel nanostructured materials and devices. To obtain specific collective properties of these […]
Dynamic and structural correlations in nanocomposites of silica with modified surface and carboxylated nitrile rubber Abstract: The sintering process of compacts of nanostructured gadolinia-doped ceria was investigated by dilatometry and by construction of the master […]
White photoluminescence emission from ZrO2 co-doped with Eu3+, Tb3+ and Tm3+ Abstract: The search for high efficiency, reliable, low power consumption and environmental friendly materials for white light-emitting diodes has become a proficient field. Single-phase […]