SEM, AFM and TEM images of LNO films sintered by (a,b,e) conventional (LNO-A) and (c,d,f) microwave (LNO-B) heating sources
Role of morphological characteristics on the conductive behavior of LaNiO3 thin films
Abstract: LaNiO3 (LNO) thin films were synthesized via the polymeric precursor method and sintered using conventional and microwave heating sources. The samples were characterized by structural morphological and electrical techniques. The crystalline structure was analyzed by X-ray diffraction and indicated rhombohedral perovskite phase in both films sintered using conventional and microwave heating. The films morphology was evaluated by scanning and transmission electron microscopy, and atomic force microscopy, and the results point out that microwave heating exerts direct influence on the morphological characteristics of LNO films contributing towards the change in the grain size distribution, porosity and roughness. Conductivity was also investigated through four-probe measurements, which pointed out a conductive and ohmic behavior of the LNO thin films prepared via the polymeric precursor method where a direct relationship was found between the morphological characteristics and the electrical properties of LNO film. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
O Laboratório Aberto de Interatividade para Disseminação do Conhecimento Científico e Tecnológico (LAbI), vinculado à Universidade Federal de São Carlos (UFSCar), é voltado à prática da divulgação científica pautada na interatividade; nas relações entre Ciência, Arte e Tecnologia.
Writers: Ricardo H. Gonçalves and Edson R. Leite Keywords: semiconductors; films; hematite ABSTRACT: Hematite is one of the most promising semiconductors used to convert solar irradiation directly into chemical energy (molecular hydrogen and oxygen) via water splitting. Although several methods […]
Writers: R.C. Gouveia and H. Kamimura and R. Munhoz and A.D. Rodrigues and E.R. Leite and A.J. Chiquito Keywords: Nanostructures; Semiconductors; Raman spectroscopy; Transport properties Abstract: Germanium nanowires have been synthesized by the well known vapor-liquid-solid growth mechanism […]
Writers: T.C. Porfirio and E.N.S. Muccillo Keywords: A. Sintering; C. Dielectric properties; D. Perovskites; E. Capacitors Abstract: The effects of small amounts of lithium fluoride sintering aid on the microstructure and dielectric properties of CaCu3Ti4O12 (CCTO) ceramics were […]